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Beilstein J. Org. Chem. 2023, 19, 212–216, doi:10.3762/bjoc.19.20
Graphical Abstract
Scheme 1: Synthesis of TAAILs. i) 1 equiv glyoxal, 2.1 equiv formaldehyde, 2 equiv NH4Cl, MeOH, 65 °C, ii) 1....
Scheme 2: Model reaction for the Friedel–Crafts acylation.
Figure 1: Time-dependent analysis of the reaction using varying amounts of anhydride. Reaction conditions: 1 ...
Scheme 3: Scope of the Friedel–Crafts acylation. Reaction conditions: 1 mmol benzene derivative, 2 equiv anhy...
Beilstein J. Org. Chem. 2018, 14, 664–671, doi:10.3762/bjoc.14.54
Scheme 1: Synthesis of complexes 2 and 3.
Figure 1: ORTEP representation of 3. Thermal ellipsoids are drawn at the 50% probability level. Selected bond...
Figure 2: UV–vis absorption spectra of complexes 2 and 3 measured in dichloromethane at room temperature.
Figure 3: Emission spectra of complexes 2 and 3 measured at room temperature and 77 K, 2 wt % in a PMMA matri...
Figure 4: Cyclic voltammograms of complexes 2 and 3, analyte concentration 10−4 M. Measured in DMF (0.1 M TBA...
Figure 5: Thin films of Pt(MPIM)(acac) left, Pt(MPIM)(mes) (2) middle, and Pt(MPIM)(dur) (3) right, 2 wt % in...
Figure 6: Photoluminescence spectra of 2 and 3 compared to the emission profile of Pt(MPIM)(acac), 2 wt % in ...
Figure 7: Localization of spin density on the complexes Pt(MPIM)(acac) left, Pt(MPIM)(mes) (2) middle, and Pt...
Beilstein J. Org. Chem. 2016, 12, 1557–1565, doi:10.3762/bjoc.12.150
Scheme 1: Synthesis of the monomethylpalladium(II) complexes 9–11 (in DCM) and 12 (in CH3CN).
Figure 1: Possible isomers.
Figure 2: ORTEP [39] style plot of complex 9 in the solid state. Thermal ellipsoids are given at the 50% probabil...
Figure 3: ORTEP [39] style plot of complex 12 in the solid state. Thermal ellipsoids are drawn at the 50% probabi...
Scheme 2: Synthesis of complex 13.
Figure 4: ORTEP [39] style plot of complex 13 in the solid state. Thermal ellipsoids are drawn at the 50% probabi...
Scheme 3: Possible pathways of methyl trifluoroacetate formation starting from complex 13.
Scheme 4: Synthesis of complex 14 by conversion of complex 13 with iodobenzene bistrifluoroacetate.
Scheme 5: Synthesis of the [((pym)^(NHC-R))PdII(CH3)2] complex 15.